2-(p-Brombenzyl)-2--buttersaeure-ethylester

Base Information

• Chemical Name: 2-(p-Brombenzyl)-2--buttersaeure-ethylester
• CAS No.: 54985-84-1
• Molecular Formula: C₁₆H₂₂BrNO₂S₂
• Molecular Weight: 404.392
• Mol file: 54985-84-1.mol

Synonyms:

Chemical Property of 2-(p-Brombenzyl)-2--buttersaeure-ethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-Brombenzyl)-2--buttersaeure-ethylester

There total 2 articles about 2-(p-Brombenzyl)-2--buttersaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl N-(ethoxycarbonylmethyl)iminodithiocarbonate (54985-61-4) + ethyl iodide (75-03-6) + 1-bromomethyl-4-bromobenzene (589-15-1) → 2-(p-Brombenzyl)-2--buttersaeure-ethylester (54985-84-1)

Guidance literature:

Multistep reaction; (i) KOtBu, THF, (ii) /BRN= 505934/;

Reference yield:

→ 2-(p-Brombenzyl)-2--buttersaeure-ethylester (54985-84-1)

Guidance literature:

N--glycinethylester (1a), 1) Ethyljodid, (CH3)3COK (-> Zwischenprodukt (nicht isoliert)), 2) p-Brombenzylbromid, (CH3)3COK;

Reference yield:

2-(p-Brombenzyl)-2--buttersaeure-ethylester (54985-84-1) → 2-(p-Bromphenyl)-2-ethylalanin-ethylester (54985-86-3)

Guidance literature:

With dihydrogen peroxide; toluene-4-sulfonic acid; In formic acid;

upstream raw materials:

dimethyl N-(ethoxycarbonylmethyl)iminodithiocarbonate

ethyl iodide

1-bromomethyl-4-bromobenzene

Downstream raw materials:

2-(p-Bromphenyl)-2-ethylalanin-ethylester