Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester

Base Information

• Chemical Name: Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester
• CAS No.: 132246-03-8
• Molecular Formula: C₂₈H₅₀N₂O₇Si₂
• Molecular Weight: 582.885

Synonyms:

Chemical Property of Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester

Chemical Property:

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Technology Process of Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester

There total 1 articles about Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-[(2R,3S)-2-Benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid (132245-95-5) → Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester (132246-03-8,132339-75-4)

Guidance literature:

With lead(IV) acetate; In N,N-dimethyl-formamide; 1) 0 deg C, 2) 0 deg C -> r.t.;

DOI:10.1016/S0040-4039(00)97182-X

Reference yield: 69.0%

Acetic acid 1-[(2R,3S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester (132246-03-8,132339-75-4) + phosphorous acid trimethyl ester (121-45-9) → [1-[(2R,3S)-2-Benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-phosphonic acid dimethyl ester (132246-09-4,132339-81-2)

Guidance literature:

With titanium tetrachloride;

DOI:10.1016/S0040-4039(00)97182-X

upstream raw materials:

2-[(2R,3S)-2-Benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid

Downstream raw materials:

[1-[(2R,3S)-2-Benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-phosphonic acid dimethyl ester

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