di(4-trifluoromethylphenyl)tindichloride

Base Information

Chemical Name:di(4-trifluoromethylphenyl)tindichloride
CAS No.:77459-83-7
Molecular Formula:C₁₄H₈Cl₂F₆Sn
Molecular Weight:479.824
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(4-trifluoromethylphenyl)tindichloride

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Technology Process of di(4-trifluoromethylphenyl)tindichloride

There total 1 articles about di(4-trifluoromethylphenyl)tindichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 402-43-7
p-trifluoromethylphenyl bromide

: 7646-78-8
tin(IV) chloride

: 77459-83-7
di(4-trifluoromethylphenyl)tindichloride

Guidance literature:: at 180 ℃; for 120h;
DOI:10.1039/c8dt03043j

Reference yield: 99.0%

: 77459-83-7
di(4-trifluoromethylphenyl)tindichloride

: 3585-33-9
lithium dimethylamide

: 952516-13-1
(p-CF₃C₆H₄)2Sn(NMe₂)2

Guidance literature:: In benzene; under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;
DOI:10.1016/j.poly.2007.06.002

Reference yield: 85.0%

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 77459-83-7
di(4-trifluoromethylphenyl)tindichloride

: cis-tin(IV)dichloride(4-trifluoromethylphenyl)(4,4'.dimethyl-2,2'-bipyridyl)

Guidance literature:: In toluene; Equimolar quantities of the starting materials in toluene are heated to boiling and mixed.; cooling to room temp., washing with light petroleum, vacuum drying, elem. anal.;