iodocarbonyl rhodium anion

Base Information

Chemical Name:iodocarbonyl rhodium anion
CAS No.:44769-94-0
Molecular Formula:C₂I₄O₂Rh
Molecular Weight:666.544
Hs Code.:

Synonyms:

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Chemical Property of iodocarbonyl rhodium anion

Chemical Property:

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Technology Process of iodocarbonyl rhodium anion

There total 1 articles about iodocarbonyl rhodium anion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-30-9
2-iodo-propane

: 95246-85-8,13986-81-7
tetraphenylarsonium dicarbonyldiiodorhodate(I)

: 44769-93-9,44769-94-0
trans-[RhI₄(CO)2]^(1-)

: (Ph₄As)[Rh(CO)(COCH(CH₃)2)I₃]

: (Ph₄As)[Rh(CO)(COC₃H₇)I₃]

Guidance literature:: In neat (no solvent); Rh-complex dissolved in neat alkyl iodide under N2; soln. heated in a stainless steel (Fisher-Porter) tube above 80°C;
DOI:10.1021/om00020a039

Reference yield: 60.0%

: 44769-94-0,44769-93-9
iodocarbonyl rhodium anion

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 603-36-1
triphenylantimony

: (rhodium)2(carbonyl)2(sulfur dioxide)3(triphenylstibine)2(iodo)2 complex

Guidance literature:: In ethanol; PPh3 addn. to SO2 treated complex soln., stay overnight at 5°C; washing (EtOH, ether), drying (vac. over CaCl2 at room temp.); elem. anal.;

Reference yield: 57.0%

: 44769-94-0,44769-93-9
iodocarbonyl rhodium anion

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 603-35-0
triphenylphosphine

: 21006-49-5,15094-66-3,87584-88-1
rhodium iodo carbonyl (triphenylphosphine)2 complex

: 167782-35-6
rhodium (sulfur dioxide)3 iodo ethanolato complex

Guidance literature:: In ethanol; PPh3 addn. to SO2 treated complex soln.; CH2Cl2 addn.(pptn.); washing (EtOH, ether), drying (vac. over CaCl2 at room temp.); elem. anal.;