vanadyltetra(p-methoxyphenyl)porphyrin

Base Information

• Chemical Name: vanadyltetra(p-methoxyphenyl)porphyrin
• CAS No.: 126635-50-5
• Molecular Formula: C₄₈H₃₆N₄O₅V
• Molecular Weight: 799.779
• Mol file: 126635-50-5.mol

Synonyms:

Chemical Property of vanadyltetra(p-methoxyphenyl)porphyrin

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of vanadyltetra(p-methoxyphenyl)porphyrin

There total 2 articles about vanadyltetra(p-methoxyphenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.8%

vanadyl acetate + 5,10,15,20-meso-tetra(p-methoxyphenyl) porphyrin → vanadyltetra(p-methoxyphenyl)porphyrin (126635-50-5)

Guidance literature:

In acetic acid; heating a mixture of 4-methoxy tetraphenyl porphyrine and VO(CH3COO)2 in glacial acetic acid at 190-200°C, 48 hours, addition to H2O, extraction with benzene and evaporation;; chromatography and recrystallization from CH3OH;;

DOI:10.1021/j150541a025

Reference yield: 20.0%

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin (22112-78-3) + vanadium(III) chloride (7718-98-1) → vanadyltetra(p-methoxyphenyl)porphyrin (126635-50-5)

Guidance literature:

In ethanol; at 179.84 ℃; for 96h; Autoclave; High pressure;

DOI:10.1002/asia.201000822

upstream raw materials:

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin

vanadium(III) chloride