C₂₀H₂₃NO₃*ClH

Base Information

• Chemical Name: C₂₀H₂₃NO₃*ClH
• CAS No.: 857436-66-9
• Molecular Formula: C₂₀H₂₃NO₃*ClH
• Molecular Weight: 361.868
• Mol file: 857436-66-9.mol

Synonyms:

Chemical Property of C₂₀H₂₃NO₃*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₂₃NO₃*ClH

There total 1 articles about C₂₀H₂₃NO₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + butanone (78-93-3) → C20H23NO3*ClH (857436-66-9)

Guidance literature:

4-methoxy-benzaldehyde; butanone; With ammonium acetate; In ethanol; for 0.25h; Heating;

With hydrogenchloride; In water;

DOI:10.1016/j.bmcl.2009.11.074

Reference yield:

C20H23NO3*ClH (857436-66-9) → 2,6-di(p-methoxyphenyl)-3-methylpiperidin-4-one (115584-11-7,138453-07-3)

Guidance literature:

With ammonia; In water; at 20 ℃; Cooling with ice;

DOI:10.1016/j.bmcl.2009.11.074

Reference yield:

C20H23NO3*ClH (857436-66-9) + thiosemicarbazide (79-19-6) → C21H26N4O2S (597577-96-3)

Guidance literature:

C₂₀H₂₃NO₃*ClH; With ammonia; In water; at 20 ℃; Cooling with ice;

thiosemicarbazide; In ethanol; for 2h; Reflux;

DOI:10.1007/s11164-010-0221-7

upstream raw materials:

4-methoxy-benzaldehyde

butanone

Downstream raw materials:

2,6-di(p-methoxyphenyl)-3-methylpiperidin-4-one

3-(2,6-bis(4-methoxyphenyl)-3-methylpiperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

C₂₁H₂₆N₄O₂S