Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

Base Information

Chemical Name:Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-
CAS No.:1089669-74-8
Molecular Formula:C₁₄H₁₃BN₂O₄S
Molecular Weight:316.145
Hs Code.:
Mol file:1089669-74-8.mol

Synonyms:

Suppliers and Price of Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

There total 5 articles about Boronic acid, B-[2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1014613-05-8
1-(benzenesulfonyl)-4-bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine

: 1089669-74-8
[2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium acetate / palladium diacetate / dichloromethane / 0.08 h / 20 °C

1.2: 20 - 65 °C

2.1: hydrogenchloride / water / 2 h / 45 °C

2.2: pH 6

With hydrogenchloride; potassium acetate; palladium diacetate; In dichloromethane; water;

Reference yield:

: 889939-25-7
1-(benzenesulfonyl)-4-bromo-1H-pyrrolo[2,3-b]pyridine

: 1089669-74-8
[2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.5 h / -35 °C

1.2: 2 h / 20 °C

2.1: potassium acetate / palladium diacetate / dichloromethane / 0.08 h / 20 °C

2.2: 20 - 65 °C

3.1: hydrogenchloride / water / 2 h / 45 °C

3.2: pH 6

With hydrogenchloride; potassium acetate; lithium diisopropyl amide; palladium diacetate; In tetrahydrofuran; n-heptane; dichloromethane; ethylbenzene; water;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1089669-74-8
[2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / 1,4-dioxane; dichloromethane; water

1.2: 120 h / 0 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.5 h / -35 °C

2.2: 2 h / 20 °C

3.1: potassium acetate / palladium diacetate / dichloromethane / 0.08 h / 20 °C

3.2: 20 - 65 °C

4.1: hydrogenchloride / water / 2 h / 45 °C

4.2: pH 6

With hydrogenchloride; sodium hydroxide; potassium acetate; tetra(n-butyl)ammonium hydrogensulfate; lithium diisopropyl amide; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; n-heptane; dichloromethane; ethylbenzene; water;