C₅₂H₄₄N₁₀O₂S₂

Base Information

• Chemical Name: C₅₂H₄₄N₁₀O₂S₂
• CAS No.: 1392495-71-4
• Molecular Formula: C₅₂H₄₄N₁₀O₂S₂
• Molecular Weight: 905.119
• Mol file: 1392495-71-4.mol

Synonyms:

Chemical Property of C₅₂H₄₄N₁₀O₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₂H₄₄N₁₀O₂S₂

There total 5 articles about C₅₂H₄₄N₁₀O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C36H32N10S2 (1392495-67-8) + 4-methoxy-benzaldehyde (123-11-5) → C52H44N10O2S2 (1392495-71-4)

Guidance literature:

With acetic acid; for 0.0833333h; Time; Temperature; Microwave irradiation;

DOI:10.1007/s11164-012-0723-6

Reference yield:

benzyl bromide (100-39-0) → C52H44N10O2S2 (1392495-71-4)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / Microwave irradiation

2: hydrazine hydrate / Microwave irradiation

3: potassium hydroxide

4: hydrazine hydrate / Microwave irradiation

5: potassium hydroxide / methanol / 0.17 h / Microwave irradiation

6: acetic acid / 0.08 h / Microwave irradiation

With potassium carbonate; hydrazine hydrate; acetic acid; potassium hydroxide; In methanol; N,N-dimethyl-formamide;

DOI:10.1007/s11164-012-0723-6

Reference yield:

1-Benzyl-1H-indole-3-carboxylic acid methyl ester (155134-26-2) → C52H44N10O2S2 (1392495-71-4)

Guidance literature:

Multi-step reaction with 5 steps

1: hydrazine hydrate / Microwave irradiation

2: potassium hydroxide

3: hydrazine hydrate / Microwave irradiation

4: potassium hydroxide / methanol / 0.17 h / Microwave irradiation

5: acetic acid / 0.08 h / Microwave irradiation

With hydrazine hydrate; acetic acid; potassium hydroxide; In methanol;

DOI:10.1007/s11164-012-0723-6

upstream raw materials:

C₃₆H₃₂N₁₀S₂

4-methoxy-benzaldehyde

benzyl bromide

1-Benzyl-1H-indole-3-carboxylic acid methyl ester