6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER

Base Information

Chemical Name:6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER
CAS No.:150401-96-0
Molecular Formula:C₁₁H₁₃NO₃
Molecular Weight:207.229
Hs Code.:
Mol file:150401-96-0.mol

Synonyms:

Suppliers and Price of 6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-(6-Methylpyridin-2-yl)-3-oxopropionic acid ethyl ester 95%
5g
$ 1568.00

A1 Biochem Labs
3-(6-Methyl-pyridin-2-yl)-3-oxo-propionicacidethylester 95%
5 g
$ 950.00

Total 5 raw suppliers

Chemical Property of 6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3-(6-Methylpyridin-2-yl)-3-oxopropionic acid ethyl ester 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER

There total 3 articles about 6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.35%

: 13602-11-4
6-methylpicolinic acid methyl ester

: 141-78-6
ethyl acetate

: 150401-96-0
ethyl 3-(6-methylpyridin-2-yl)-3-oxopropanoate

Guidance literature:: ethyl acetate; With sodium ethanolate; In toluene; at 20 ℃; for 1h;

6-methylpicolinic acid methyl ester; In toluene; at 25 - 95 ℃; for 15h;

Reference yield:

: 39640-51-2
ethyl 6-methylpyridine-2-carboxylate

: 141-78-6
ethyl acetate

: 150401-96-0
ethyl 3-(6-methylpyridin-2-yl)-3-oxopropanoate

Guidance literature:: ethyl acetate; With sodium ethanolate; In toluene; at 20 ℃; for 1h; Inert atmosphere;

ethyl 6-methylpyridine-2-carboxylate; In toluene; for 20h; Inert atmosphere; Reflux;

Reference yield:

: 934-60-1
6-methyl-2-pyridinecarboxylic acid

: 150401-96-0
ethyl 3-(6-methylpyridin-2-yl)-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / water / 24 h / pH 9 / Reflux

2.1: sodium ethanolate / toluene / 1 h / 20 °C / Inert atmosphere

2.2: 20 h / Inert atmosphere; Reflux

With sulfuric acid; sodium ethanolate; In water; toluene;