(2R,3R)-1,2,3,4-Tetrachlorobutane

Base Information

• Chemical Name: (2R,3R)-1,2,3,4-Tetrachlorobutane
• CAS No.: 52134-24-4
• Molecular Formula: C₄H₆Cl₄
• Molecular Weight: 195.904
• DSSTox Substance ID: DTXSID301026313
• Nikkaji Number: J231.783D
• Mol file: 52134-24-4.mol

Synonyms:52134-24-4;rel-(2R,3R)-1,2,3,4-Tetrachlorobutane;(2R,3R)-1,2,3,4-Tetrachlorobutane;DTXSID301026313

Chemical Property of (2R,3R)-1,2,3,4-Tetrachlorobutane

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 195.919411
• Heavy Atom Count: 8
• Complexity: 48

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(C(C(CCl)Cl)Cl)Cl
• Isomeric SMILES: C([C@H]([C@@H](CCl)Cl)Cl)Cl

Technology Process of (2R,3R)-1,2,3,4-Tetrachlorobutane

There total 12 articles about (2R,3R)-1,2,3,4-Tetrachlorobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-1,4-dichlorobut-2-ene (110-57-6) → meso-1,2,3,4-tetrachlorobutane (28507-96-2) + racem.-1,2,3,4-Tetrachlorbutan (3405-32-1,28507-96-2,52134-24-4) + (2S,3S)-1,2,4-Trichloro-3-methoxy-butane (76465-31-1,76465-32-2,76951-33-2,76951-34-3) + (2S,3R)-1,2,4-Trichloro-3-methoxy-butane (76465-31-1,76465-32-2,76951-33-2,76951-34-3)

Guidance literature:

With chlorine; In dichloromethane; at -20 ℃; Further byproducts given;

Reference yield:

methanol (67-56-1) + 3,4-dichlorobut-1-ene (310447-99-5,310448-01-2,64037-54-3) → meso-1,2,3,4-tetrachlorobutane (28507-96-2) + racem.-1,2,3,4-Tetrachlorbutan (3405-32-1,28507-96-2,52134-24-4) + (2R,3R)-1,2,3-Trichloro-4-methoxy-butane (76465-33-3,76465-34-4,76951-37-6,76951-38-7) + (2R,3S)-1,2,3-Trichloro-4-methoxy-butane (76465-33-3,76465-34-4,76951-37-6,76951-38-7)

Guidance literature:

With chlorine; at -20 ℃; Further byproducts given;

Reference yield:

methanol (67-56-1) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → meso-1,2,3,4-tetrachlorobutane (28507-96-2) + racem.-1,2,3,4-Tetrachlorbutan (3405-32-1,28507-96-2,52134-24-4) + (2S,3S)-1,2,4-Trichloro-3-methoxy-butane (76465-31-1,76465-32-2,76951-33-2,76951-34-3) + (2R,3S)-1,2,3-Trichloro-4-methoxy-butane (76465-33-3,76465-34-4,76951-37-6,76951-38-7)

Guidance literature:

In dichloromethane; at -20 ℃; Further byproducts given;

upstream raw materials:

1,4-Dichloro-2-butyne

methanol

3,4-dichlorobut-1-ene

trans-1,4-dichlorobut-2-ene

Downstream raw materials:

2,3-dichlorobuta-1,3-diene

perfluoro-1,2,3,4-tetrachlorobutane