C₃₂H₄₄N₆O₉S

Base Information

Chemical Name:C₃₂H₄₄N₆O₉S
CAS No.:274901-49-4
Molecular Formula:C₃₂H₄₄N₆O₉S
Molecular Weight:688.802
Hs Code.:

C<sub>32</sub>H<sub>44</sub>N<sub>6</sub>O<sub>9</sub>S

Synonyms:

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Chemical Property of C₃₂H₄₄N₆O₉S

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Technology Process of C₃₂H₄₄N₆O₉S

There total 9 articles about C₃₂H₄₄N₆O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2480-93-5
Boc-Orn(Z)-OH

: 274901-49-4
C₃₂H₄₄N₆O₉S

Guidance literature:: Multi-step reaction with 10 steps

1.1: ethyl chloroformate / tetrahydrofuran / 0.25 h / -10 - 0 °C

1.2: 83 percent / NaBH₄ / tetrahydrofuran; methanol / 0 °C

2.1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

3.1: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

4.1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

5.1: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

6.1: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

7.1: hydrogen / 10percent Pd/C / ethanol / 4 h

8.1: 230 mg / tetrahydrofuran

9.1: TFA / CH₂Cl₂ / 0.5 h / 0 °C

10.1: 81 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; chloroformic acid ethyl ester; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Substitution / 1.2: Reduction / 2.1: Substitution / 3.1: Substitution / 4.1: Deacetylation / 5.1: Substitution / 6.1: Oxidation / 7.1: Hydrogenolysis / 8.1: Substitution / 9.1: Hydrolysis / 10.1: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 105562-75-2
N²-(tert-butyloxycarbonyl)-N⁵-(benzyloxycarbonyl)-2(S),5-diaminopentanol

: 274901-49-4
C₃₂H₄₄N₆O₉S

Guidance literature:: Multi-step reaction with 9 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

3: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

4: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

5: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

6: hydrogen / 10percent Pd/C / ethanol / 4 h

7: 230 mg / tetrahydrofuran

8: TFA / CH₂Cl₂ / 0.5 h / 0 °C

9: 81 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Substitution / 3: Deacetylation / 4: Substitution / 5: Oxidation / 6: Hydrogenolysis / 7: Substitution / 8: Hydrolysis / 9: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 233689-90-2
Boc-NH-CH((CH₂)3NHZ)-CH₂-S-CO-CH₃

: 274901-49-4
C₃₂H₄₄N₆O₉S

Guidance literature:: Multi-step reaction with 7 steps

1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

2: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

3: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

4: hydrogen / 10percent Pd/C / ethanol / 4 h

5: 230 mg / tetrahydrofuran

6: TFA / CH₂Cl₂ / 0.5 h / 0 °C

7: 81 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile; 1: Deacetylation / 2: Substitution / 3: Oxidation / 4: Hydrogenolysis / 5: Substitution / 6: Hydrolysis / 7: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P