tetramesityldibismuthane

Base Information

Chemical Name:tetramesityldibismuthane
CAS No.:165904-00-7
Molecular Formula:C₃₆H₄₄Bi₂
Molecular Weight:894.706
Hs Code.:

Synonyms:

Suppliers and Price of tetramesityldibismuthane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramesityldibismuthane

Chemical Property:

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Technology Process of tetramesityldibismuthane

There total 3 articles about tetramesityldibismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 146498-75-1
chlorobis(2,4,6-trimethylphenyl)bismuthane

: 165904-00-7
tetramesityldibismuthane

Guidance literature:: With LiBH₄; In diethyl ether; byproducts: H2; all manipulations under Ar atm.; LiBH4 added to cooled soln. of Mes2BiCl(-70°C), mixt. slowly warmed to -40°C with vigorous stirr ing, filtered at this temp. then stirred at 0°C for 2 h; concd. in vac., cooled to -28°C;
DOI:10.1515/znb-2005-0209

Reference yield: 52.6%

: 1277-43-6,78206-33-4
cobaltocene

: 156488-39-0
dimesitylbismuth(III) bromide

: 165904-00-7
tetramesityldibismuthane

Guidance literature:: In tetrahydrofuran; Ar atm., absence of light; molar ratio R2BiBr:CoCp2 2:1, room temp., stirring (1 h); decantation, evapn.; elem. anal.;

Reference yield: 40.7%

: 156488-39-0
dimesitylbismuth(III) bromide

: 7440-23-5
sodium

: 165904-00-7
tetramesityldibismuthane

Guidance literature:: In ammonia; byproducts: NaBr; NH3 (liquid); Ar atm., absence of light; equimolar ratio, cooling (-60°C), stirring (2 h); evapn., washing (PhMe), elem. anal.;