Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

Base Information

Chemical Name:Bis(3-diphenylphosphanopropyl)tert.-butylphosphan
CAS No.:107164-43-2
Molecular Formula:C₃₄H₄₁P₃
Molecular Weight:542.621
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

Chemical Property:

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Technology Process of Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

There total 1 articles about Bis(3-diphenylphosphanopropyl)tert.-butylphosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 29949-76-6
diallyl-tert-butylphosphane

: 829-85-6
diphenylphosphane

: 107164-43-2
Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

Guidance literature:: With 2,2'-azobis(isobutyronitrile); for 70h; Irradiation;

Reference yield:

: diμ-chlorotetrakis(η2-cyclooctene)diiridium(I)

: 107164-43-2
Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

: 154798-15-9
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chloroiridium(I)

Guidance literature:: In hexane; toluene; prepd. from Ir2Cl2(cyclo-C8H14)4 and the tris(phosphine) at room temp. in toluene/hexane in the cold;
DOI:10.1016/0022-328X(93)83430-4

Reference yield:

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 107164-43-2
Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

Guidance literature:: In toluene; under inert gas atmosphere; stirring of a soln. of the Rh-compd. and the phosphane in toluene for 2 h at room temp.; pptd. crystals are filtered off, washed with hexane and dried in vac.; partial evapn. of solvent from mother liquor and pptn. with hexane yields further Rh-complex; elem. anal.;