4-methoxyphenyl 1-naphthoate

Base Information

Chemical Name:4-methoxyphenyl 1-naphthoate
CAS No.:443663-97-6
Molecular Formula:C₁₈H₁₄O₃
Molecular Weight:278.307
Hs Code.:
Mol file:443663-97-6.mol

Synonyms:

Suppliers and Price of 4-methoxyphenyl 1-naphthoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxyphenyl 1-naphthoate

Chemical Property:

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Technology Process of 4-methoxyphenyl 1-naphthoate

There total 3 articles about 4-methoxyphenyl 1-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 90-15-3
α-naphthol

: 201230-82-2
carbon monoxide

: 66107-29-7
4-methoxyphenyl triflate

: 443663-97-6
4-methoxyphenyl 1-naphthoate

Guidance literature:: With palladium diacetate; potassium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In N,N-dimethyl acetamide; at 90 ℃; for 48h; under 2250.23 Torr;
DOI:10.1016/j.jcat.2020.06.034

Reference yield:

: 201230-82-2
carbon monoxide

: 150-76-5
4-methoxy-phenol

: 90555-42-3
1-naphtyldimethylsulfonium trifluoromethanesulfonate

: 443663-97-6
4-methoxyphenyl 1-naphthoate

Guidance literature:: With C₃₉H₃₂OP₂*C₁₃H₁₂N^(1-)*Pd⁽²⁺⁾*CH₃O₃S^(1-); N-ethyl-N,N-diisopropylamine; In toluene; at 110 ℃; for 12h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/acs.orglett.9b00067

Reference yield:

: 10075-72-6
1-(methylthio)naphthalene

: 443663-97-6
4-methoxyphenyl 1-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / 12 h / 65 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; C₃₉H₃₂OP₂*C₁₃H₁₂N^(1-)*Pd⁽²⁺⁾*CH₃O₃S^(1-) / toluene / 12 h / 110 °C / 760.05 Torr / Inert atmosphere

With C₃₉H₃₂OP₂*C₁₃H₁₂N^(1-)*Pd⁽²⁺⁾*CH₃O₃S^(1-); N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/acs.orglett.9b00067