bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

Base Information

Chemical Name:bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium
CAS No.:263910-94-7
Molecular Formula:C₅₀H₅₈N₂O₄P₂Ru
Molecular Weight:914.039
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

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Technology Process of bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

There total 1 articles about bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 124-38-9,18923-20-1
carbon dioxide

: diisopropylammonium [Ru2Cl2(μ-Cl)3(PPh3)4]

: 108-18-9
diisopropylamine

: 263910-94-7
bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

Guidance literature:: In toluene; byproducts: diisopropylammonium chloride; amine added under CO2 to a soln. of Ru complex in toluene, mixt. stirredat ambient temp. for 4 d; filtered, filtrate evapd. to dryness under vac., residue suspended in heptane, solid filtered off and dried under vac.;

Reference yield:

: 263910-94-7
bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

: 1333-74-0
hydrogen

: 114595-94-7
RuH₂(H₂)(PPh₃)3

Guidance literature:: In toluene; soln. of Ru compd. in toluene stirred under H2 at 80°C for 4 h; not isolated, detected by NMR spectroscopy;

Reference yield:

: 263910-94-7
bis(N,N-diisopropylcarbamato)bis(triphenylphosphine)ruthenium

: 1333-74-0
hydrogen

: 603-35-0
triphenylphosphine

: 114595-94-7
RuH₂(H₂)(PPh₃)3

Guidance literature:: In toluene; soln. of Ru compd. and PPh3 (1 equiv.) in toluene treated with H2, heatdat 80°C for 24 h; not isolated, detected by NMR spectroscopy;