Cyclohexanecarbamic acid 1,1-bis(p-fluorophenyl)-2-propynyl ester

Base Information

• Chemical Name: Cyclohexanecarbamic acid 1,1-bis(p-fluorophenyl)-2-propynyl ester
• CAS No.: 10087-77-1
• Molecular Formula: C₂₂H₂₁F₂NO₂
• Molecular Weight: 369.411
• Hs Code.: 2924299090
• Mol file: 10087-77-1.mol

Synonyms:Cyclohexanecarbamicacid, 1,1-bis(p-fluorophenyl)-2-propynyl ester (8CI); 2-Propyn-1-ol,1,1-bis(p-fluorophenyl)-, cyclohexanecarbamate (8CI)

Chemical Property of Cyclohexanecarbamic acid 1,1-bis(p-fluorophenyl)-2-propynyl ester

Chemical Property:

• Vapor Pressure: 3.68E-09mmHg at 25°C
• Boiling Point: 474.2°C at 760 mmHg
• PKA: 11.23±0.20(Predicted)
• Flash Point: 240.6°C
• PSA: 41.82000
• Density: 1.22g/cm³
• LogP: 5.10490

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarbamic acid 1,1-bis(p-fluorophenyl)-2-propynyl ester

There total 2 articles about Cyclohexanecarbamic acid 1,1-bis(p-fluorophenyl)-2-propynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-bis(4-fluorophenyl)prop-2-yn-1-ol (357-77-7) + cyclohexylamine (108-91-8,157973-60-9) + phenyl chloroformate (1885-14-9) → N-Cyclohexyl-carbamidsaeure-<1,1-bis-(4-fluor-phenyl)-propin-(2)-ylester> (10087-77-1)

Guidance literature:

Multistep reaction; (i) Py, CH₂Cl₂, (ii) /BRN= 471175/, Et₂O;

DOI:10.1021/jm00313a008

Reference yield:

→ N-Cyclohexyl-carbamidsaeure-<1,1-bis-(4-fluor-phenyl)-propin-(2)-ylester> (10087-77-1)

Guidance literature:

/BRN= 850808/, 1.) ClCOOPh, 2.) Cyclohexylamin;

upstream raw materials:

1,1-bis(4-fluorophenyl)prop-2-yn-1-ol

cyclohexylamine

phenyl chloroformate

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