η6-pyridinetricarbonylchromium

Base Information

Chemical Name:η6-pyridinetricarbonylchromium
CAS No.:125963-05-5
Molecular Formula:C₈H₅CrNO₃
Molecular Weight:215.129
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of η6-pyridinetricarbonylchromium

Chemical Property:

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Technology Process of η6-pyridinetricarbonylchromium

There total 1 articles about η6-pyridinetricarbonylchromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 180985-82-4,125963-05-5
η6-pyridinetricarbonylchromium

: 201230-82-2
carbon monoxide

: 14740-77-3
pentacarbonyl(pyridine)chromium⁽⁰⁾

: 70906-46-6
(η(1)-C5H5N)Cr(CO)4

: 125963-05-5,180985-82-4
(η(1)-C5H5N)Cr(CO)3

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

Guidance literature:: In solid matrix; Irradiation (UV/VIS); CH4 / CO (10 : 1) solid matrix; irradn. (λ = 460 , 250 nm); detd. by IR spectroscopy;
DOI:10.1021/om960090+

Reference yield: 100.0%

: 180985-82-4,125963-05-5
η6-pyridinetricarbonylchromium

: 917-54-4
methyllithium

: 100-39-0
benzyl bromide

: N-benzyl-exo-2-methyl-1,2-dihydropyridine(tricarbonyl)chromium

Guidance literature:: In tetrahydrofuran; N2; -78°C; 1.1-1.2 equiv. alkyllithium added; stirred for 2-3 h; ecxess of benzyl bromide added; warmed to room temp.; stirred for 24 h;; evapd.; extd. with CH2Cl2; evapd.; chromd. (light petroleum/ether 2/3); elem. anal.;;
DOI:10.1039/P19910000757

Reference yield: 35.0%

: 180985-82-4,125963-05-5
η6-pyridinetricarbonylchromium

: 591-51-5
phenyllithium

: N-methyl exo-2-phenyl-1,2-dihydropyridinetricarbonylchromium

Guidance literature:: With methyl iodide; In tetrahydrofuran; N2; -78°C; 1.1-1.2 equiv. alkyllithium added; stirred for 2-3 h; ecxess of MeI added; warmed to room temp.; stirred for 24 h;; evapd.; extd. with CH2Cl2; evapd.; chromd. (light petroleum/ether 1/1); crystd. from CH2Cl2/hexane; elem. anal.;;
DOI:10.1039/P19910000757