Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

Base Information

Chemical Name:Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)
CAS No.:80448-77-7
Molecular Formula:C₅₂H₄₄ClO₂P₄Rh₂*F₆P
Molecular Weight:1211.04
Hs Code.:

Rh<sub>2</sub>(CO)2Cl((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>

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Chemical Property of Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

Chemical Property:

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Technology Process of Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

There total 1 articles about Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: (Rh₂(H)(CO)3((C₆H₅)2PCH₂P(C₆H₅)2)2)⁽¹⁺⁾*PF₆^(1-)*CH₂Cl₂=(Rh₂(H)(CO)3((C₆H₅)2PCH₂P(C₆H₅)2)2)PF₆*CH₂Cl₂

: C₅₃H₄₄ClO₃P₄Rh₂⁽¹⁺⁾

: 80448-77-7
Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: In dichloromethane; byproducts: H2; 1 drop of conc. HCl was added to a soln. of complex; replacing a gas phase with N2, pptn. with Et2O; elem. anal.;

Reference yield:

: 288-13-1
NH-pyrazole

: 80448-77-7
Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

: {Rh2(μ-bis(diphenylphosphino)methane)2(CO)2(μ-pyrazolate)}(PF6)

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; hexane; react. of pyrazole in THF with BuLi in hexane, addn. to Rh-complex in THF, stirring; concg., addn. of Et2O;

Reference yield:

: 7554-65-6
4-methyl-1H-pyrazole

: 80448-77-7
Rh₂(CO)2Cl((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)

: {Rh2(μ-bis(diphenylphosphino)methane)2(CO)2(μ-4-methylpyrazolate)}(PF6)

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; hexane; react. of pyrazole derivative in THF with BuLi in hexane, addn. to Rh-complex in THF, stirring; concg., addn. of Et2O;