tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾

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Chemical Name:tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾
CAS No.:74005-17-7
Molecular Formula:C₂₅H₃₄MoO₄P₂Si₂
Molecular Weight:612.601
Hs Code.:

tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum<sup>(0)</sup>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾

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Technology Process of tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾

There total 4 articles about tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 65060-48-2
cis-(PhPHSiMe₃)2(CO)4

: 109-64-8
1,3-dibromo-propane

: 74005-17-7
tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾

Guidance literature:: With MeLi; In diethyl ether; byproducts: LiBr; soln. of MeLi added to soln. of Mo-compd. at -78°C, stirred at 20°C for 2 h, Br-compd. dropped at -10°C, stirred at 20°C for 48 h, volatile compds. removed at 20°C/0.1 Torr, CH2Cl2added to residue; LiBr centrifuged, concd., decompd. with petroleum ether;

Reference yield: 77.0%

: 75-77-4
chloro-trimethyl-silane

: 74005-16-6,152784-45-7,152784-44-6
tetracarbonyl[1,3-bis(phenylphosphino)propane]molybdenum⁽⁰⁾

: 917-54-4
methyllithium

: 74005-17-7
tetracarbonyl(1,3-bis[phenyl(trimethylsilyl)phosphino]propane)molybdenum⁽⁰⁾

Guidance literature:: In diethyl ether; byproducts: LiCl; soln. of Mo-compd. and MeLi decompd. with soln. of Me3SiCl at -78°C, stirred at 20°C overnight, volatile compds. removed, CH2Cl2 added to residue; centrifuged, CH2Cl2 removed, crystd. from n-pentane at -40°C; elem. anal.;