(5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one

Base Information

• Chemical Name: (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one
• CAS No.: 105086-96-2
• Molecular Formula: C₃₂H₃₈O₅S
• Molecular Weight: 534.717

Synonyms:

Chemical Property of (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one

There total 3 articles about (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenyldisulfane (882-33-7) → (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one (105086-96-2)

Guidance literature:

DOI:10.1021/jo00374a050

Reference yield:

(E)-3-(6-Formyl-6-methyl-cyclohex-2-enyl)-but-2-enoic acid methyl ester (98993-13-6,99094-70-9,111138-05-7) → (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one (105086-96-2)

Guidance literature:

DOI:10.1021/jo00374a050

Reference yield:

(1R,2R)-1-Methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbaldehyde (104995-47-3) + (5S,10S)-10-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-1-oxa-spiro[4.5]deca-3,7-dien-2-one (104995-48-4) → (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one (104995-49-5) + (5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one (105086-96-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/jo00374a050

upstream raw materials:

(1R,2R)-1-Methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbaldehyde

(5S,10S)-10-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-1-oxa-spiro[4.5]deca-3,7-dien-2-one

(E)-3-(6-Formyl-6-methyl-cyclohex-2-enyl)-but-2-enoic acid methyl ester

diphenyldisulfane

Downstream raw materials:

Toluene-4-sulfonic acid (E)-3-{(5R,6R)-3-[(1S,2S)-2-((E)-3-benzenesulfonyl-1-methyl-propenyl)-1-methyl-cyclohex-3-enecarbonyl]-4-methoxy-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-allyl ester

Toluene-4-sulfonic acid (E)-3-{(5R,6R)-4-methoxy-3-[(1S,2S)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-allyl ester

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