iodorhodium (III) tetra-p-tolylporphyrin

Base Information

Chemical Name:iodorhodium (III) tetra-p-tolylporphyrin
CAS No.:103533-53-5
Molecular Formula:C₄₈H₃₆IN₄Rh
Molecular Weight:898.651
Hs Code.:

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Chemical Property of iodorhodium (III) tetra-p-tolylporphyrin

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Technology Process of iodorhodium (III) tetra-p-tolylporphyrin

There total 2 articles about iodorhodium (III) tetra-p-tolylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 591-50-4
iodobenzene

: Rh₂(tetra-p-tolylporphyrinato)₂

: 103533-53-5
iodorhodium (III) tetra-p-tolylporphyrin

: 911206-97-8
5,10,15,20-tetra(p-tolyl)porphyrinato-rhodium(III)-phenyl

Guidance literature:: In benzene; at 120 ℃; for 0.0833333h; Inert atmosphere; Darkness;
DOI:10.1021/om300441p

Reference yield: 18.0%

: 591-50-4
iodobenzene

: 205259-72-9
rhodium(III) tetrakis(4-tolyl)porphyrin chloride

: 103533-53-5
iodorhodium (III) tetra-p-tolylporphyrin

: 911206-97-8
5,10,15,20-tetra(p-tolyl)porphyrinato-rhodium(III)-phenyl

Guidance literature:: With potassium acetate; tert-butyl alcohol; In benzene; at 120 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1021/om300441p

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 103533-53-5
iodorhodium (III) tetra-p-tolylporphyrin

: Rh(C₁₂H₉N)4CHICO₂C₂H₅

Guidance literature:: In dichloromethane-d2; placing Rh-complex soln. in NMR tube, sealing (rubber septum), cooling to -78°C, org. compd. addn. via syringe, soln. mixing; tube placing in 0°C ice bath for 30 min; NMR spectroscopy;
DOI:10.1021/ja00058a007