N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

Base Information

Chemical Name:N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride
CAS No.:1356146-69-4
Molecular Formula:C₄₅H₆₄N₇O₈*Cl
Molecular Weight:866.498
Hs Code.:

N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

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Chemical Property of N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

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Technology Process of N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

There total 6 articles about N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1356146-83-2
1-azido-17-isocyano-3,6,9,12,15-pentaoxaheptadecane

: 81-88-9
rhodamine B

: 75-31-0
isopropylamine

: 1356146-69-4
N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

Guidance literature:: In methanol; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1039/c1ob06581e

Reference yield:

: 109789-40-4
3,6,9,12,15-pentaoxaheptadecane-1,17-diyl dimethanesulfonate

: 1356146-69-4
N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide; sodium hydrogencarbonate / water / 12 h / 80 °C

2.1: phosphoric acid; triphenylphosphine / diethyl ether / 24 h / 0 - 20 °C

2.2: 24 h / 0 °C

3.1: 3 h / Reflux

4.1: diisopropylamine; trichlorophosphate / dichloromethane / 2 h / 0 - 20 °C

5.1: methanol / 1 h / 100 °C / Microwave irradiation

With sodium azide; phosphoric acid; sodium hydrogencarbonate; diisopropylamine; triphenylphosphine; trichlorophosphate; In methanol; diethyl ether; dichloromethane; water; 2.1: Staudinger reaction / 5.1: Ugi condensation;
DOI:10.1039/c1ob06581e

Reference yield:

: 2615-15-8
pentaethylene glycol

: 1356146-69-4
N-[9-(2-[(2'-azido-2-oxo-6,9,12,15,18-pentaoxa-3-azaicos-1-yl)(1-methylethyl)carbamoyl]phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 4 h / 0 - 20 °C

2.1: sodium azide; sodium hydrogencarbonate / water / 12 h / 80 °C

3.1: phosphoric acid; triphenylphosphine / diethyl ether / 24 h / 0 - 20 °C

3.2: 24 h / 0 °C

4.1: 3 h / Reflux

5.1: diisopropylamine; trichlorophosphate / dichloromethane / 2 h / 0 - 20 °C

6.1: methanol / 1 h / 100 °C / Microwave irradiation

With sodium azide; phosphoric acid; sodium hydrogencarbonate; diisopropylamine; triphenylphosphine; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; 3.1: Staudinger reaction / 6.1: Ugi condensation;
DOI:10.1039/c1ob06581e