acetoxy-2-chlorocyclohex-2-ene

Base Information

• Chemical Name: acetoxy-2-chlorocyclohex-2-ene
• CAS No.: 67820-31-9
• Molecular Formula: C₈H₁₁ClO₂
• Molecular Weight: 174.627
• Mol file: 67820-31-9.mol

Synonyms:

Chemical Property of acetoxy-2-chlorocyclohex-2-ene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetoxy-2-chlorocyclohex-2-ene

There total 4 articles about acetoxy-2-chlorocyclohex-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylselenyl chloride (5707-04-0) + rac-3-acetoxycyclohexene (76644-52-5,76704-31-9,14447-34-8,62247-41-0) → cis acetoxy-2-chlorocyclohex-3-ene + acetoxy-2-chlorocyclohex-2-ene (67820-31-9) + acetoxy-3-chlorocyclohex-2-ene (109392-23-6) + trans acetoxy-2-chlorocyclohex-3-ene

Guidance literature:

Phenylselenyl chloride; rac-3-acetoxycyclohexene; With zinc(II) chloride; In chloroform; at 20 ℃;

With dihydrogen peroxide; In chloroform; at 20 ℃;

With 2,6-dichloro-benzonitrile; In tetrachloromethane; Title compound not separated from byproducts; Heating;

DOI:10.1016/j.tet.2004.05.084

Reference yield:

1-chlorocyclohexene (930-66-5) + potassium acetate (127-08-2) → acetoxy-2-chlorocyclohex-2-ene (67820-31-9)

Guidance literature:

With acetic acid; (anodic oxidation);

DOI:10.1246/bcsj.51.2179

Reference yield:

1-chlorocyclohexene (930-66-5) → acetoxy-2-chlorocyclohex-2-ene (67820-31-9)

Guidance literature:

With selenium(IV) oxide; acetic anhydride; acetic acid;

upstream raw materials:

1-chlorocyclohexene

potassium acetate

selenium(IV) oxide

acetic anhydride

Downstream raw materials:

2-chlorocyclohex-2-en-1-ol