C₄₂H₆₆O₇Si₂

Base Information

Chemical Name:C₄₂H₆₆O₇Si₂
CAS No.:1429410-46-7
Molecular Formula:C₄₂H₆₆O₇Si₂
Molecular Weight:739.153
Hs Code.:

C<sub>42</sub>H<sub>66</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₄₂H₆₆O₇Si₂

Chemical Property:

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Technology Process of C₄₂H₆₆O₇Si₂

There total 8 articles about C₄₂H₆₆O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51674-10-3
N,N-diethyl-2-methoxybenzamide

: 1429410-46-7
C₄₂H₆₆O₇Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1.5 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 °C

2.1: potassium cyanide; 18-crown-6 ether / dichloromethane / 2 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

3.2: 1.08 h / Inert atmosphere

With potassium cyanide; 18-crown-6 ether; potassium tert-butylate; tert.-butyl lithium; In tetrahydrofuran; dichloromethane; pentane; 3.1: |Hauser-Kraus Annulation / 3.2: |Hauser-Kraus Annulation;
DOI:10.1021/ol400686f

Reference yield:

: 1161160-10-6
ethyl (5R)-5-hydroxyhex-2-ynoate

: 1429410-46-7
C₄₂H₆₆O₇Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 15 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 2 h / -78 °C / Inert atmosphere

4.1: potassium carbonate / water / 0.5 h

4.2: 0 - 20 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

5.2: 1.08 h / Inert atmosphere

With 1H-imidazole; n-butyllithium; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; potassium carbonate; In tetrahydrofuran; hexane; dichloromethane; water; ethyl acetate; 4.1: |Horner-Wadsworth-Emmons Olefination / 4.2: |Horner-Wadsworth-Emmons Olefination / 5.1: |Hauser-Kraus Annulation / 5.2: |Hauser-Kraus Annulation;
DOI:10.1021/ol400686f

Reference yield:

: 579-75-9
2-Methoxybenzoic acid

: 1429410-46-7
C₄₂H₆₆O₇Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / ethyl acetate / 5 h

2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1.5 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 °C

3.1: potassium cyanide; 18-crown-6 ether / dichloromethane / 2 h / 0 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

4.2: 1.08 h / Inert atmosphere

With potassium cyanide; 1-hydroxy-pyrrolidine-2,5-dione; 18-crown-6 ether; potassium tert-butylate; tert.-butyl lithium; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; ethyl acetate; pentane; 4.1: |Hauser-Kraus Annulation / 4.2: |Hauser-Kraus Annulation;
DOI:10.1021/ol400686f