methyl (4-methoxyphenyl)glyoxylate phenylhydrazone

Base Information

Chemical Name:methyl (4-methoxyphenyl)glyoxylate phenylhydrazone
CAS No.:75600-94-1
Molecular Formula:C₁₆H₁₆N₂O₃
Molecular Weight:284.315
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (4-methoxyphenyl)glyoxylate phenylhydrazone

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Technology Process of methyl (4-methoxyphenyl)glyoxylate phenylhydrazone

There total 1 articles about methyl (4-methoxyphenyl)glyoxylate phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23786-14-3
4-methoxy-phenyl acetic acid methyl ester

: 100-63-0
phenylhydrazine

: 75600-94-1
methyl (4-methoxyphenyl)glyoxylate phenylhydrazone

Guidance literature:: With acetic acid; In ethanol; for 1h; Yield given; Heating;
DOI:10.1021/jo00314a018

Reference yield:

: 75600-94-1
methyl (4-methoxyphenyl)glyoxylate phenylhydrazone

: 75601-16-0
3-(4-acetaminophenyl)-4-methoxyphenylglyoxylate 4-nitrophenylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / polyphosporic acid / 1 h / 100 - 120 °C

2: HCl / methanol / 2 h / Heating

3: acetic acid / Heating

With hydrogenchloride; polyphosporic acid; In methanol; acetic acid;
DOI:10.1021/jo00314a018