C₃₁H₄₂O₃S₂

Base Information

Chemical Name:C₃₁H₄₂O₃S₂
CAS No.:1454583-64-2
Molecular Formula:C₃₁H₄₂O₃S₂
Molecular Weight:526.805
Hs Code.:

C<sub>31</sub>H<sub>42</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₁H₄₂O₃S₂

Chemical Property:

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Technology Process of C₃₁H₄₂O₃S₂

There total 9 articles about C₃₁H₄₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117286-10-9
undecylmagnesium bromide

: 1454583-64-2
C₃₁H₄₂O₃S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 15 h / Reflux

2.1: N-Bromosuccinimide / tetrahydrofuran / 15 h / 25 °C

3.1: magnesium / tetrahydrofuran / 0.5 h / Reflux

3.2: 15 h / Reflux

4.1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C

5.1: potassium carbonate / acetonitrile / 6 h / Reflux

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C

7.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C

With N-Bromosuccinimide; osmium(VIII) oxide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); pyridinium p-toluenesulfonate; boron tribromide; potassium carbonate; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile; 1.1: |Kumada Cross-Coupling / 3.2: |Kumada Cross-Coupling;
DOI:10.1039/c3sc50664a

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1454583-64-2
C₃₁H₄₂O₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / 1,2-dimethoxyethane; water / 15 h / Reflux

2.1: magnesium / tetrahydrofuran / 0.5 h / Reflux

2.2: 15 h / Reflux

3.1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C

4.1: potassium carbonate / acetonitrile / 6 h / Reflux

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C

6.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C

With osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyridinium p-toluenesulfonate; boron tribromide; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetone; acetonitrile; 1.1: |Suzuki Coupling / 2.2: |Kumada Cross-Coupling;
DOI:10.1039/c3sc50664a

Reference yield:

: 358718-72-6
C₁₅H₂₅BrS

: 1454583-64-2
C₃₁H₄₂O₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 0.5 h / Reflux

1.2: 15 h / Reflux

2.1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C

3.1: potassium carbonate / acetonitrile / 6 h / Reflux

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C

5.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C

With osmium(VIII) oxide; pyridinium p-toluenesulfonate; boron tribromide; potassium carbonate; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile; 1.2: |Kumada Cross-Coupling;
DOI:10.1039/c3sc50664a