Technology Process of C15H12FNO
There total 5 articles about C15H12FNO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate; methanol / 18 h / 20 °C
2: hydrogen bromide / chloroform / 2 h / 20 °C
3: boron tribromide / dichloromethane / 21 h / -78 - 20 °C
4: N,N-dimethyl-formamide / 72 h / 20 °C
5: potassium carbonate / N,N-dimethyl-formamide
With
methanol; sodium tetrahydroborate; hydrogen bromide; boron tribromide; potassium carbonate;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron tribromide / dichloromethane / 21 h / -78 - 20 °C
2: N,N-dimethyl-formamide / 72 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide
With
boron tribromide; potassium carbonate;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide / chloroform / 2 h / 20 °C
2: boron tribromide / dichloromethane / 21 h / -78 - 20 °C
3: N,N-dimethyl-formamide / 72 h / 20 °C
4: potassium carbonate / N,N-dimethyl-formamide
With
hydrogen bromide; boron tribromide; potassium carbonate;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;