2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate

Base Information

Chemical Name:2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate
CAS No.:678166-63-7
Molecular Formula:C₂₁H₂₄N₂O₅S
Molecular Weight:416.498
Hs Code.:

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Chemical Property of 2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate

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Technology Process of 2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate

There total 2 articles about 2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119244-91-6
(3-benzyloxycarbonylamino-2-hydroxypropyl)-carbamic acid benzyl ester

: 507-09-5
tiolacetic acid

: 678166-63-7
2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at -10 - 20 ℃; for 21h;
DOI:10.1055/s-2003-44382

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 678166-63-7
2-(benzyloxycarbonyl)amino-1-(benzyloxycarbonyl)aminomethylethyl thioacetate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / CH₂Cl₂ / 20 °C

2: diethyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 21 h / -10 - 20 °C

With sodium hydroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2003-44382