Technology Process of Benzenepropanoic acid, a-ethenyl-, methyl ester
There total 21 articles about Benzenepropanoic acid, a-ethenyl-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,4,5,5-tetramethyl-2-(4-phenylbut-2-en-1-yl)-1,3,2-dioxaborolane;
With
potassium tert-butylate; triphenylphosphine; bis(pinacol)diborane; copper dichloride;
In
methanol;
at 20 ℃;
for 1.5h;
Inert atmosphere;
Schlenk technique;
carbon dioxide;
With
potassium tert-butylate;
at 70 ℃;
for 24h;
under 760.051 Torr;
Inert atmosphere;
Schlenk technique;
methyl iodide;
at 60 ℃;
for 3h;
Reagent/catalyst;
regioselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/d0cc05056c
- Guidance literature:
-
(E)-buta-1,3-dienylbenzene;
With
methanol; potassium tert-butylate; triphenylphosphine; bis(pinacol)diborane; copper dichloride;
at 20 ℃;
for 1.5h;
Inert atmosphere;
Schlenk technique;
carbon dioxide;
With
potassium tert-butylate;
at 70 ℃;
for 24h;
under 760.051 Torr;
Inert atmosphere;
Schlenk technique;
methyl iodide;
at 60 ℃;
for 3h;
regioselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/d0cc05056c
- Guidance literature:
-
With
sulfuric acid;
for 2h;
Heating;
