Technology Process of C11H11(2)H3O
There total 5 articles about C11H11(2)H3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium deuteride;
In
tetrahydrofuran;
for 24h;
DOI:10.1021/jo0005518
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2.5 g / p-TsOH / Heating
2: 85 percent / LiAlD4; AlCl3 / diethyl ether
3: LiCl; 2,6-dimethylpyridine; CH3SO2Cl / dimethylformamide / 12 h / 0 °C
4: LiAlD4 / tetrahydrofuran / 24 h
With
2,6-dimethylpyridine; aluminium trichloride; lithium aluminium deuteride; toluene-4-sulfonic acid; methanesulfonyl chloride; lithium chloride;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo0005518
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethyl phosphite; NaH / 1,2-dimethoxy-ethane / 0 °C
1.2: 1,2-dimethoxy-ethane / 1 h / 20 °C
2.1: 2.5 g / p-TsOH / Heating
3.1: 85 percent / LiAlD4; AlCl3 / diethyl ether
4.1: LiCl; 2,6-dimethylpyridine; CH3SO2Cl / dimethylformamide / 12 h / 0 °C
5.1: LiAlD4 / tetrahydrofuran / 24 h
With
2,6-dimethylpyridine; aluminium trichloride; lithium aluminium deuteride; Diethyl phosphonate; sodium hydride; toluene-4-sulfonic acid; methanesulfonyl chloride; lithium chloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; N,N-dimethyl-formamide;
1.1: Ylide formation / 1.2: Horner-Wittig reaction;
DOI:10.1021/jo0005518
