[(triphenylphosphine)2Ag(O₂COH)]

Base Information

Chemical Name:[(triphenylphosphine)2Ag(O₂COH)]
CAS No.:1313762-32-1
Molecular Formula:C₃₇H₃₁AgO₃P₂
Molecular Weight:693.467
Hs Code.:

[(triphenylphosphine)2Ag(O<sub>2</sub>COH)]

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Chemical Property of [(triphenylphosphine)2Ag(O₂COH)]

Chemical Property:

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Technology Process of [(triphenylphosphine)2Ag(O₂COH)]

There total 2 articles about [(triphenylphosphine)2Ag(O₂COH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 144-55-8
sodium hydrogencarbonate

: silver nitrate

: 603-35-0
triphenylphosphine

: 1313762-32-1
[(triphenylphosphine)2Ag(O₂COH)]

Guidance literature:: In ethanol; water; byproducts: NO3(1-); to a boiling soln. of PPh3 (6.0 mmol) in EtOH was added with stirring a hot soln. of AgNO3 (3.0 mmol) in H2O; the hot soln. was immediately added with stirring to a soln. of NaHCO3 (12.5 mmol) in H2O at ambient temp.; stirring until cooling; compd. was collected by vac. filtration and washed with 1:1 EtOH/H2O; itwas dissolved in CH3CN by stirring and heating to 75°C in a wate r bath; resulting soln. was filtered while hot; crystals were dried withfilter paper; elem. anal.;
DOI:10.1039/c1dt10416k

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 7732-18-5
water

: 603-35-0
triphenylphosphine

: silver carbonate

: 1313762-32-1
[(triphenylphosphine)2Ag(O₂COH)]

Guidance literature:: In neat (no solvent, solid phase); Ag-contg. compd. (0.25 mmol) and PPh3 (1.0 mmol) were ground together with a mortar and pestle, first dry and then after addn. of EtOH; the process was repeated 6 times with addn. of EtOH; the paste obtained was allowed to dry in air; IR spectra studies;
DOI:10.1039/c1dt10416k