1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

Base Information

Chemical Name:1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane
CAS No.:158919-65-4
Molecular Formula:C₂₃H₃₂O₆
Molecular Weight:404.503
Hs Code.:

Synonyms:

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Chemical Property of 1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

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Technology Process of 1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

There total 6 articles about 1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 67-56-1
methanol

: 158919-73-4
1,3-bis<4-(bromomethyl)-2,5-dimethoxyphenyl>propane

: 158919-65-4
1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

Guidance literature:: With sodium methylate; for 3h; Heating;

Reference yield:

: 10365-11-4
1,3-bis(2,5-dimethoxyphenyl)propan-1-one

: 158919-65-4
1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / H₂, p-TsOH*H₂O / 10percent Pd/C / methanol / 3 h

2: 85 percent / 33percent HBr / acetic acid; CCl₄ / 1 h

3: 85 percent / NaOMe / 3 h / Heating

With hydrogen bromide; hydrogen; sodium methylate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; tetrachloromethane; acetic acid;

Reference yield:

: 1201-38-3
2',5'-dimethoxyacetophenone

: 158919-65-4
1,3-bis<2,5-dimethoxy-4-(methoxymethyl)phenyl>propane

Guidance literature:: Multi-step reaction with 5 steps

1: NaOMe / methanol / 1.) 40 deg C, 2 h, 2.) room temp., 12 h

2: 75 percent / H₂ / 5percent Pd/C / ethyl acetate / 2 h

3: 89 percent / H₂, p-TsOH*H₂O / 10percent Pd/C / methanol / 3 h

4: 85 percent / 33percent HBr / acetic acid; CCl₄ / 1 h

5: 85 percent / NaOMe / 3 h / Heating

With hydrogen bromide; hydrogen; sodium methylate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; tetrachloromethane; acetic acid; ethyl acetate;