isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone

Base Information

• Chemical Name: isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone
• CAS No.: 76128-47-7
• Molecular Formula: C₁₈H₂₀N₄
• Molecular Weight: 292.384
• Mol file: 76128-47-7.mol

Synonyms:

Chemical Property of isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone

There total 1 articles about isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

isobutyraldehyde (78-84-2) + (1-benzyl-2-benzimidazolyl)hydrazine (14180-45-1) → isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone (76128-47-7)

Guidance literature:

In isopropyl alcohol; for 0.0833333h; Heating;

DOI:10.1007/BF00513171

Reference yield: 60.0%

isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone (76128-47-7) → isopropyl-1-benzyl-2-benzimidazolylazoketoxime (76128-55-7)

Guidance literature:

With n-Amyl nitrite; at 20 ℃; for 24h;

DOI:10.1007/BF00513171

Reference yield:

2-hydroxy-4-nitroaniline diazonium salt + isobutyraldehyde 1-benzyl-2-benzimidazolylhydrazone (76128-47-7) → C24H23N7O3

Guidance literature:

In water; isopropyl alcohol; for 0.666667h; Yield given; pH of mixture ca. 9;

upstream raw materials:

isobutyraldehyde

(1-benzyl-2-benzimidazolyl)hydrazine

Downstream raw materials:

isopropyl-1-benzyl-2-benzimidazolylazoketoxime