fucoxanthin 3-acetate 5'-trimethylsilyl ether

Base Information

• Chemical Name: fucoxanthin 3-acetate 5'-trimethylsilyl ether
• CAS No.: 143932-66-5
• Molecular Formula: C₄₇H₆₈O₇Si
• Molecular Weight: 773.138
• Mol file: 143932-66-5.mol

Synonyms:

Chemical Property of fucoxanthin 3-acetate 5'-trimethylsilyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of fucoxanthin 3-acetate 5'-trimethylsilyl ether

There total 1 articles about fucoxanthin 3-acetate 5'-trimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

chloro-trimethyl-silane (75-77-4) + fucoxanthin monoacetate (3351-87-9) → fucoxanthin 3-acetate 5'-trimethylsilyl ether (143932-66-5)

Guidance literature:

With pyridine; 1,1,1,2,2,2-hexamethyldisilane; for 24h;

Reference yield:

fucoxanthin 3-acetate 5'-trimethylsilyl ether (143932-66-5) + methyl iodide (74-88-4) → fucoxanthin 3-acetate 5'-trimethylsilyl ether hemiketal

Guidance literature:

With water; sodium hydride; Yield given. Multistep reaction; 1.) THF, 30 min;

Reference yield:

fucoxanthin 3-acetate 5'-trimethylsilyl ether (143932-66-5) + methyl iodide (74-88-4) → fucoxanthin 3-acetate 5'-trimethylsilyl ether methyl ketal

Guidance literature:

With sodium hydride; Multistep reaction; 1.) THF, 5 min, 2.) THF, 4 h;

upstream raw materials:

chloro-trimethyl-silane

fucoxanthin monoacetate

Refernces