acetic benzoic thioanhydride

Base Information

• Chemical Name: acetic benzoic thioanhydride
• CAS No.: 26555-24-8
• Molecular Formula: C₉H₈O₂S
• Molecular Weight: 180.227
• Mol file: 26555-24-8.mol

Synonyms:

Chemical Property of acetic benzoic thioanhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic benzoic thioanhydride

There total 4 articles about acetic benzoic thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzoyl chloride (98-88-4) + zinc thiolacetate → acetic benzoic thioanhydride (26555-24-8)

Guidance literature:

In dichloromethane; for 36h; Heating;

DOI:10.1016/0040-4020(95)00044-9

Reference yield: 81.0%

Benzoyl bromide (618-32-6) + zinc thiolacetate → acetic benzoic thioanhydride (26555-24-8)

Guidance literature:

In dichloromethane; for 20h; Heating;

DOI:10.1016/0040-4020(95)00044-9

Reference yield: 32.0%

thiobenzoic acid (98-91-9) + acetyl chloride (75-36-5) → acetic benzoic thioanhydride (26555-24-8)

Guidance literature:

With sodium hydride; 1.) 2 h, benzene, 2.) 4 h, ether, -15 deg C;

upstream raw materials:

thiobenzoic acid potassium salt

acetyl chloride

thiobenzoic acid

Benzoyl bromide

Downstream raw materials:

1'-acetyl-2β,3β-dihydro-5α-androst-2-eno<2,3-b>azirin-17-one ethylene acetal

1'-benzoyl-2β,3β-dihydro-5α-androst-2-eno<2,3-b>azirin-17-one ethylene acetal

benzoyl-phenyl-disulfane

benzoylsulfenyl chloride