1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

Base Information

Chemical Name:1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine
CAS No.:79328-99-7
Molecular Formula:C₂₅H₂₆N₂O₅S
Molecular Weight:466.558
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

Chemical Property:

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Technology Process of 1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

There total 6 articles about 1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-86-1
pyridine

: 79328-99-7
1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / NaBH₄ / ethanol / 1.5 h / -78 °C

2: 73 percent / 96 h / 100 °C

3: Me₃SiI / CH₂Cl₂

4: p-TsOH / tetrahydrofuran / 16 h / Ambient temperature

With sodium tetrahydroborate; trimethylsilyl iodide; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00337a003

Reference yield:

: 79328-85-1
N-benzyloxycarbonyl-1,2-dihydropyridine

: 79328-99-7
1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / 96 h / 100 °C

2: Me₃SiI / CH₂Cl₂

3: p-TsOH / tetrahydrofuran / 16 h / Ambient temperature

With trimethylsilyl iodide; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00337a003

Reference yield:

: 79328-88-4
methyl 2-(benzyloxycarbonyl)-7-exo-(1-phenylsulfonylindol-2-yl)-2-azabicyclo[2.2.2]oct-5-ene-7-endo-carboxylate

: 79328-99-7
1-benzenesulfonyl-6-nor-15-methoxy-15,20-dihydro-20-deethylcatharantine

Guidance literature:: Multi-step reaction with 2 steps

1: Me₃SiI / CH₂Cl₂

2: p-TsOH / tetrahydrofuran / 16 h / Ambient temperature

With trimethylsilyl iodide; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00337a003