C₄₆H₆₅ClN₄O₅

Base Information

Chemical Name:C₄₆H₆₅ClN₄O₅
CAS No.:1449796-62-6
Molecular Formula:C₄₆H₆₅ClN₄O₅
Molecular Weight:789.499
Hs Code.:

C<sub>46</sub>H<sub>65</sub>ClN<sub>4</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₄₆H₆₅ClN₄O₅

Chemical Property:

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Technology Process of C₄₆H₆₅ClN₄O₅

There total 20 articles about C₄₆H₆₅ClN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 1449796-62-6
C₄₆H₆₅ClN₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane

2: Lawessons reagent / toluene

3: acetic acid; silver benzoate / dichloromethane

4: water; sodium hydroxide / methanol; tetrahydrofuran

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

6: trifluoroacetic acid / dichloromethane

With Lawessons reagent; dmap; water; silver benzoate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 473-98-3
betulin

: 1449796-62-6
C₄₆H₆₅ClN₄O₅

Guidance literature:: Multi-step reaction with 15 steps

1: 3 h / 100 °C

2: acetic anhydride; hydrogen bromide / toluene; acetic acid / 1.5 h / 105 °C

3: acetic anhydride; acetic acid; sodium acetate; sodium dichromate dihydrate / toluene / 60 °C

4: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

5: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C

6: triethylamine / 20 °C

7: toluene-4-sulfonic acid / 20 °C

8: sodium tetrahydroborate; methanol / 1 h / 20 °C

9: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

10: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

11: hydrazine hydrate / dichloromethane / 0.5 h / 0 °C

12: acetic acid; silver benzoate / dichloromethane

13: water; sodium hydroxide / methanol; tetrahydrofuran

14: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

15: trifluoroacetic acid / dichloromethane

With methanol; dmap; sodium tetrahydroborate; oxalyl dichloride; sodium dichromate dihydrate; water; hydrogen bromide; sodium acetate; silver benzoate; acetic anhydride; silica gel; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; toluene;

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 1449796-62-6
C₄₆H₆₅ClN₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: triethylamine / dichloromethane

3: Lawessons reagent / toluene

4: acetic acid; silver benzoate / dichloromethane

5: water; sodium hydroxide / methanol; tetrahydrofuran

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

7: trifluoroacetic acid / dichloromethane

With Lawessons reagent; dmap; oxalyl dichloride; water; silver benzoate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;