Technology Process of C23H17N5S
There total 7 articles about C23H17N5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / water / 40 h / Reflux
2.1: trichlorophosphate / 2 h / 105 °C
3.1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C
3.2: 14 h
4.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; N,N-dimethyl-formamide / Inert atmosphere; Microwave irradiation; Heating
With
bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0); triethylamine; trichlorophosphate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.6b00117
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trichlorophosphate / 2 h / 105 °C
2.1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C
2.2: 14 h
3.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; N,N-dimethyl-formamide / Inert atmosphere; Microwave irradiation; Heating
With
bis-triphenylphosphine-palladium(II) chloride; triethylamine; trichlorophosphate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.6b00117
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / 80 °C
1.2: 1.25 h / 80 °C
2.1: acetic acid / water / 0.5 h / 35 °C
3.1: tetrakis(triphenylphosphine) palladium(0) / water / 40 h / Reflux
4.1: trichlorophosphate / 2 h / 105 °C
5.1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C
5.2: 14 h
6.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; N,N-dimethyl-formamide / Inert atmosphere; Microwave irradiation; Heating
With
bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0); acetic acid; triethylamine; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.6b00117