Technology Process of C22H32FN3O5S
There total 5 articles about C22H32FN3O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
formic acid; C26H40FN3O6S;
at 20 ℃;
for 24h;
With
N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline;
In
chloroform;
at 20 ℃;
for 24h;
DOI:10.1002/psc.2414
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
2.1: water; sodium hydroxide / methanol / 0 - 20 °C
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
4.1: 24 h / 20 °C
4.2: 24 h / 20 °C
With
water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
methanol; dichloromethane;
DOI:10.1002/psc.2414
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water; sodium hydroxide / methanol / 0 - 20 °C
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
3.1: 24 h / 20 °C
3.2: 24 h / 20 °C
With
water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
methanol; dichloromethane;
DOI:10.1002/psc.2414