C₂₂H₃₂O₅

Base Information

Chemical Name:C₂₂H₃₂O₅
CAS No.:122131-32-2
Molecular Formula:C₂₂H₃₂O₅
Molecular Weight:376.493
Hs Code.:

C<sub>22</sub>H<sub>32</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₂H₃₂O₅

Chemical Property:

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Technology Process of C₂₂H₃₂O₅

There total 16 articles about C₂₂H₃₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 122131-32-2
C₂₂H₃₂O₅

Guidance literature:: Multi-step reaction with 12 steps

2: 92 percent / LDA / tetrahydrofuran / 0.04 h / -78 °C

3: 75 percent / 1) LDA, 2) CF₃COOH / tetrahydrofuran / -78 °C

4: 83 percent / LiAlH₄ / tetrahydrofuran / -30 °C

5: 95 percent / pyridine

6: 92 percent / NaH / tetrahydrofuran

7: 1) Zn-Cu, 2) Zn, NH₄Cl / 1) ether, room temperature, 5.5 h; 2) MeOH, 0 deg C

8: 74 percent / methanol / Ambient temperature

9: NaBH₄ / methanol

10: 1) MsCl, pyridine; 2) t-BuOK / 2) DMSO

11: 89 percent / HgCl₂ / acetonitrile; H₂O / 40 °C

12: TsOH

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; copper; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; methanesulfonyl chloride; trifluoroacetic acid; mercury dichloride; zinc; lithium diisopropyl amide; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1016/S0040-4039(00)82126-7

Reference yield:

: 116217-06-2
(3aR,4R,7aS)-2-Oxo-2,3,3a,4,5,7a-hexahydro-benzofuran-4-carboxylic acid

: 122131-32-2
C₂₂H₃₂O₅

Guidance literature:: Multi-step reaction with 12 steps

2: 92 percent / LDA / tetrahydrofuran / 0.04 h / -78 °C

3: 75 percent / 1) LDA, 2) CF₃COOH / tetrahydrofuran / -78 °C

4: 83 percent / LiAlH₄ / tetrahydrofuran / -30 °C

5: 95 percent / pyridine

6: 92 percent / NaH / tetrahydrofuran

7: 1) Zn-Cu, 2) Zn, NH₄Cl / 1) ether, room temperature, 5.5 h; 2) MeOH, 0 deg C

8: 74 percent / methanol / Ambient temperature

9: NaBH₄ / methanol

10: 1) MsCl, pyridine; 2) t-BuOK / 2) DMSO

11: 89 percent / HgCl₂ / acetonitrile; H₂O / 40 °C

12: TsOH

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; copper; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; methanesulfonyl chloride; trifluoroacetic acid; mercury dichloride; zinc; lithium diisopropyl amide; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1016/S0040-4039(00)82126-7

Reference yield:

: 74320-39-1
methyl cis-6-<2-(dimethylamino)-2-oxoethyl>-3-cyclohexene-1-carboxylate

: 122131-32-2
C₂₂H₃₂O₅

Guidance literature:: Multi-step reaction with 15 steps

1: 1) LiOH, 2) KI₃, aq. NaHCO₃ / 1) aq. MeOH

2: 92 percent / DBU / benzene

3: 1) BF₃*OEt₂, 2) 10percent HCl / 1) CH₂Cl₂; 2) THF, reflux

5: 92 percent / LDA / tetrahydrofuran / 0.04 h / -78 °C

6: 75 percent / 1) LDA, 2) CF₃COOH / tetrahydrofuran / -78 °C

7: 83 percent / LiAlH₄ / tetrahydrofuran / -30 °C

8: 95 percent / pyridine

9: 92 percent / NaH / tetrahydrofuran

10: 1) Zn-Cu, 2) Zn, NH₄Cl / 1) ether, room temperature, 5.5 h; 2) MeOH, 0 deg C

11: 74 percent / methanol / Ambient temperature

12: NaBH₄ / methanol

13: 1) MsCl, pyridine; 2) t-BuOK / 2) DMSO

14: 89 percent / HgCl₂ / acetonitrile; H₂O / 40 °C

15: TsOH

With pyridine; hydrogenchloride; lithium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium triiodide; boron trifluoride diethyl etherate; potassium tert-butylate; copper; sodium hydride; sodium hydrogencarbonate; ammonium chloride; toluene-4-sulfonic acid; methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; mercury dichloride; zinc; lithium diisopropyl amide; In tetrahydrofuran; methanol; water; acetonitrile; benzene;
DOI:10.1016/S0040-4039(00)82126-7