2,5-Dimercapto-1,4-phenylendimethanol

Base Information

Chemical Name:2,5-Dimercapto-1,4-phenylendimethanol
CAS No.:154822-13-6
Molecular Formula:C₈H₁₀O₂S₂
Molecular Weight:202.298
Hs Code.:

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Chemical Property of 2,5-Dimercapto-1,4-phenylendimethanol

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Technology Process of 2,5-Dimercapto-1,4-phenylendimethanol

There total 3 articles about 2,5-Dimercapto-1,4-phenylendimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 25906-67-6
2,5-bis(dimethylthiocarbamoylsulfanyl)terephthalic acid diethyl ester

: 154822-13-6
2,5-Dimercapto-1,4-phenylendimethanol

Guidance literature:: With lithium aluminium tetrahydride;

Reference yield:

: 5870-38-2
diethyl 2,5-(dihydroxy)terephthalate

: 154822-13-6
2,5-Dimercapto-1,4-phenylendimethanol

Guidance literature:: Multi-step reaction with 3 steps

1: DABCO / dimethylformamide / Ambient temperature

2: diphenyl ether / 225 - 230 °C

3: 95 percent / LiAlH₄

With 1,4-diaza-bicyclo[2.2.2]octane; lithium aluminium tetrahydride; In diphenylether; N,N-dimethyl-formamide;

Reference yield:

: 25906-63-2
2,5-bis(dimethylthiocarbamoyloxy)terephthalic acid diethyl ester

: 154822-13-6
2,5-Dimercapto-1,4-phenylendimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl ether / 225 - 230 °C

2: 95 percent / LiAlH₄

With lithium aluminium tetrahydride; In diphenylether;