2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

Base Information

Chemical Name:2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon
CAS No.:77798-64-2
Molecular Formula:C₃₀H₄₆N₂O₁₀
Molecular Weight:594.703
Hs Code.:

Synonyms:

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Chemical Property of 2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

Chemical Property:

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Technology Process of 2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

There total 6 articles about 2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 77798-61-9
2,5-Bis(11-carboxyundecyl)hydrochinon-diacetat

: 77798-64-2
2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

Guidance literature:: With nitric acid; In propionic acid; for 240h; Ambient temperature;

Reference yield:

: 1108-58-3
<10-(Methoxycarbonyl)decyl>triphenylphosphoniumiodid

: 77798-64-2
2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

Guidance literature:: Multi-step reaction with 6 steps

1: NaOMe / dimethylformamide / 1) 0 deg C, 10 min, 2) r.t., 1.5 h

2: 70 percent / dimethylformamide / 3 h / Ambient temperature

3: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

4: 48percent HBr / acetic acid / 14 h / 110 °C

5: pyridine / 14 h / Ambient temperature

6: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

With hydrogen bromide; hydrogen; nitric acid; sodium methylate; nickel; In pyridine; methanol; acetic acid; propionic acid; N,N-dimethyl-formamide;

Reference yield:

: 77798-57-3
2,5-Bis(11-methoxycarbonyl-1-undecenyl)hydrochinon-dimethylether

: 77798-64-2
2,5-Bis(11-carboxyundecyl)-3,6-dinitro-1,4-benzochinon

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

2: 48percent HBr / acetic acid / 14 h / 110 °C

3: pyridine / 14 h / Ambient temperature

4: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

With hydrogen bromide; hydrogen; nitric acid; nickel; In pyridine; methanol; acetic acid; propionic acid;