4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide
CAS No.:611180-20-2
Molecular Formula:C₁₆H₁₈N₄O₂S
Molecular Weight:330.411
Hs Code.:

4-methyl-<i>N</i>-(1,5,7-trimethyl-1<i>H</i>-imidazo[4,5-<i>b</i>]pyridin-2-yl)-benzenesulfonamide

Synonyms:

Suppliers and Price of 4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

There total 6 articles about 4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89856-44-0
2-amino-5-bromo-4,6-dimethylpyridine

: 611180-20-2
4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / potassium nitrate; concd. sulfuric acid / 1 h / 20 °C

2: 98 percent / hydrogen; ammonium hydroxide / palladium on carbon / methanol / 18 h / 50 °C / 2585.74 Torr

3: 49 percent / potassium carbonate / acetone / 18 h / 20 °C

4: lithium aluminum hydride / tetrahydrofuran / 1 h / Heating

5: 477 mg / CH₂Cl₂ / 1 h / 40 °C

With ammonium hydroxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; potassium carbonate; potassium nitrate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570400403

Reference yield:

: 89791-76-4
2-amino-3-nitro-4,6-dimethyl-5-bromo-pyridine

: 611180-20-2
4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / hydrogen; ammonium hydroxide / palladium on carbon / methanol / 18 h / 50 °C / 2585.74 Torr

2: 49 percent / potassium carbonate / acetone / 18 h / 20 °C

3: lithium aluminum hydride / tetrahydrofuran / 1 h / Heating

4: 477 mg / CH₂Cl₂ / 1 h / 40 °C

With ammonium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570400403

Reference yield:

: 5407-87-4
2-Amino-4,6-dimethylpyridine

: 611180-20-2
4-methyl-N-(1,5,7-trimethyl-1H-imidazo[4,5-b]pyridin-2-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 59 percent / bromine; glacial acetic acid / 1.33 h / 20 °C

2: 64 percent / potassium nitrate; concd. sulfuric acid / 1 h / 20 °C

3: 98 percent / hydrogen; ammonium hydroxide / palladium on carbon / methanol / 18 h / 50 °C / 2585.74 Torr

4: 49 percent / potassium carbonate / acetone / 18 h / 20 °C

5: lithium aluminum hydride / tetrahydrofuran / 1 h / Heating

6: 477 mg / CH₂Cl₂ / 1 h / 40 °C

With ammonium hydroxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; bromine; potassium carbonate; acetic acid; potassium nitrate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570400403