Technology Process of C40H44N4O4
There total 14 articles about C40H44N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1021/jm401536b
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: potassium carbonate / acetonitrile
2.1: n-butyllithium / tetrahydrofuran
3.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / 760.05 Torr
3.2: 0.25 h / 20 °C
3.3: 3 h / Reflux
4.1: nitric acid; acetic acid / 0.5 h / 70 °C
5.1: tin(II) chloride dihdyrate; hydrogenchloride / ethanol / 3 h / 80 °C
6.1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 13 h / 0 - 20 °C
7.1: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C
8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
9.1: triphenylphosphine; carbon tetrabromide / dichloromethane
10.1: triethylamine / N,N-dimethyl-formamide / 20 °C
With
hydrogenchloride; n-butyllithium; tert.-butylnitrite; tin(II) chloride dihdyrate; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; carbon tetrabromide; trimethylsilylazide; palladium on activated charcoal; tetrabutyl ammonium fluoride; hydrogen; nitric acid; potassium carbonate; acetic acid; triethylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
7.1: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 13 h / 0 - 20 °C
2: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
4: triphenylphosphine; carbon tetrabromide / dichloromethane
5: triethylamine / N,N-dimethyl-formamide / 20 °C
With
tert.-butylnitrite; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; carbon tetrabromide; trimethylsilylazide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
2: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b