chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

Base Information

Chemical Name:chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]
CAS No.:1429426-51-6
Molecular Formula:C₄₅H₄₆AuBClF₂N₄O₂P
Molecular Weight:987.087
Hs Code.:

chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

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Chemical Property of chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

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Technology Process of chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

There total 6 articles about chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1429426-48-1
4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene

: 1429426-51-6
chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

Guidance literature:: In benzene; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c2dt32055j

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1429426-51-6
chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; triethylamine / acetonitrile / 72 h / Inert atmosphere; Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: triethylamine / chloroform / 19 h / Inert atmosphere; Reflux

4: benzene / 4 h / 20 °C / Inert atmosphere

With palladium diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; chloroform; acetonitrile; benzene;
DOI:10.1039/c2dt32055j

Reference yield:

: 829-85-6
diphenylphosphane

: 1429426-51-6
chloro[(4,4-difluoro-8-(4-((2-(4-(diphenylphosphino)benzamido)ethyl)carbamoyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene)gold(I)]

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; triethylamine / acetonitrile / 72 h / Inert atmosphere; Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: triethylamine / chloroform / 19 h / Inert atmosphere; Reflux

4: benzene / 4 h / 20 °C / Inert atmosphere

With palladium diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; chloroform; acetonitrile; benzene;
DOI:10.1039/c2dt32055j