Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2⁽¹⁺⁾*(Cl₃Ga)2N(CH₂CH₃)2^(1-)={Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2}{(Cl₃Ga)2N(CH₂CH₃)2}

Base Information

• Chemical Name: Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2⁽¹⁺⁾*(Cl₃Ga)2N(CH₂CH₃)2^(1-)={Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2}{(Cl₃Ga)2N(CH₂CH₃)2}
• CAS No.: 136546-95-7
• Molecular Formula: C₄H₁₀Cl₆Ga₂N*C₁₀H₂₆Cl₂GaN₂Si
• Molecular Weight: 767.338
• Mol file: 136546-95-7.mol

Synonyms:

Chemical Property of Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2⁽¹⁺⁾*(Cl₃Ga)2N(CH₂CH₃)2^(1-)={Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2}{(Cl₃Ga)2N(CH₂CH₃)2}

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2⁽¹⁺⁾*(Cl₃Ga)2N(CH₂CH₃)2^(1-)={Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2}{(Cl₃Ga)2N(CH₂CH₃)2}

There total 1 articles about Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2⁽¹⁺⁾*(Cl₃Ga)2N(CH₂CH₃)2^(1-)={Cl₂Ga(N(CH₂CH₃)2)2Si(CH₃)2}{(Cl₃Ga)2N(CH₂CH₃)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.9%

bis(diethylamino)dimethylsilane (4669-59-4) + Gallium trichloride (13450-90-3) → Cl2Ga(N(CH2CH3)2)2Si(CH3)2(1+)*(Cl3Ga)2N(CH2CH3)2(1-)={Cl2Ga(N(CH2CH3)2)2Si(CH3)2}{(Cl3Ga)2N(CH2CH3)2} (136546-95-7) + (N,N-diethylamino)dimethylchlorosilane (6026-02-4)

Guidance literature:

In diethyl ether; GaCl3 was dissolved in diethyl ether, stirred soln. was cooled in an ice bath, addn. of the silane, the soln. was refluxed for 7 h, pptn., all steps under N2 or Ar; the liquid portion was removed from the solid by vacuum distn., the solid was recrystd. (CH2Cl2), elem. anal.;

upstream raw materials:

bis(diethylamino)dimethylsilane

Gallium trichloride