(3-Chloropropyl)methoxydimethylsilane

Base Information

• Chemical Name: (3-Chloropropyl)methoxydimethylsilane
• CAS No.: 18171-14-7
• Molecular Formula: C6H15ClOSi
• Molecular Weight: 166.723
• Hs Code.: 2931900090
• European Community (EC) Number: 242-055-5
• DSSTox Substance ID: DTXSID20171180
• Nikkaji Number: J260.908H
• Wikidata: Q83041269
• Mol file: 18171-14-7.mol

Synonyms:18171-14-7;3-CHLOROPROPYLDIMETHYLMETHOXYSILANE;(3-Chloropropyl)methoxydimethylsilane;3-chloropropyl-methoxy-dimethylsilane;(3-Chloropropyl)(methoxy)dimethylsilane;Silane, (3-chloropropyl)methoxydimethyl-;3-Chloropropyl Dimethyl Methoxysilane;EINECS 242-055-5;C6H15ClOSi;Dimethyl(3-chloropropyl)methoxysilane;(3-Chloropropyl)dimethylmethoxysilane;SCHEMBL56148;CH3OSi(CH3)2(CH2)3Cl;DTXSID20171180;3-chloropropyldimethylmethoxy-silane;MFCD00270987;3-Chloropropyl Dimethyl Methoxylsilane;AKOS006378567;(3-Chloropropyl)(methoxy)dimethylsilane #;CS-0448626;FT-0615524;A880975

Chemical Property of (3-Chloropropyl)methoxydimethylsilane

Chemical Property:

• Vapor Pressure: 6.45mmHg at 25°C
• Melting Point: <0°C
• Refractive Index: 1.4278
• Boiling Point: 144.3 °C at 760 mmHg
• Flash Point: 36.1 °C
• PSA: 9.23000
• Density: 0,94 g/cm3
• LogP: 2.46680
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 166.0580693
• Heavy Atom Count: 9
• Complexity: 75.5

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Statements: 10-36/37/38
• Safety Statements: 16-26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CO[Si](C)(C)CCCCl

Technology Process of (3-Chloropropyl)methoxydimethylsilane

There total 4 articles about (3-Chloropropyl)methoxydimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methanol (67-56-1) + (3-chloropropyl)dimethylchlorosilane (10605-40-0) → γ-chloropropylmethoxydimethylsilane (18171-14-7)

Guidance literature:

With triethylamine; In diethyl ether; for 5h; Heating;

DOI:10.1021/ja034691l

Reference yield: 95.0%

methylmagnesium bromide (75-16-1) + 3-Chloropropyltrimethoxysilan (2530-87-2) → γ-chloropropylmethoxydimethylsilane (18171-14-7)

Guidance literature:

In diethyl ether;

DOI:10.1016/S0040-4039(00)80078-7

Reference yield: 85.0%

methanol (67-56-1) + chloropropyl(dimethyl)ethoxysilane (13508-63-9) → chloropropyl dimethylsilanol (174476-90-5) + γ-chloropropylmethoxydimethylsilane (18171-14-7) + 1,3-bis<3-chloropropyl>-1,1,3,3-tetramethyldisiloxane (18132-72-4)

Guidance literature:

methanol; chloropropyl(dimethyl)ethoxysilane; With sodium hydroxide; In methanol; water; at 20 ℃; for 1.5h;

With potassium dihydrogenphosphate; at 20 ℃; pH=7;

upstream raw materials:

methanol

(3-chloropropyl)dimethylchlorosilane

methylmagnesium bromide

3-Chloropropyltrimethoxysilan

Downstream raw materials:

(N-aminoethyl)aminopropylmethoxydimethylsilane

[4-({3-[(3-Chloro-propyl)-dimethyl-silanyl]-propyl}-dimethyl-silanyl)-phenyl]-dimethyl-amine

(4-{[3-({3-[(3-Chloro-propyl)-dimethyl-silanyl]-propyl}-dimethyl-silanyl)-propyl]-dimethyl-silanyl}-phenyl)-dimethyl-amine

{4-[(3-Iodo-propyl)-dimethyl-silanyl]-phenyl}-dimethyl-amine