Technology Process of C5H2BrCl2NO
There total 2 articles about C5H2BrCl2NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Acetyl bromide;
at 80 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide; acetic anhydride / water / 54 h / 20 - 60 °C
2: sulfuric acid; nitric acid / 1.5 h / 100 °C
3: Acetyl bromide / 0.17 h / 80 °C
With
Acetyl bromide; sulfuric acid; dihydrogen peroxide; nitric acid; acetic anhydride;
In
water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; benzene / 16 h / 80 °C / Heating / reflux
2: phosphorus trichloride / dichloromethane / 0.17 h / 20 °C
3: methanol; sodium hydroxide; water / 16 h / Heating / reflux
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide) / 16 h / 20 °C
5: 1H-tetrazole / dichloromethane; acetonitrile / 16 h / 20 °C
6: tert.-butylhydroperoxide / dichloromethane; acetonitrile / 0.33 h / 0 °C
7: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
With
1H-tetrazole; hydrogenchloride; methanol; tert.-butylhydroperoxide; sodium hydroxide; water; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; phosphorus trichloride;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; DMF (N,N-dimethyl-formamide); dichloromethane; water; acetonitrile; benzene;