ethyl 9H-fluorene-1-carboxylate

Base Information

• Chemical Name: ethyl 9H-fluorene-1-carboxylate
• CAS No.: 81699-50-5
• Molecular Formula: C₁₆H₁₄O₂
• Molecular Weight: 238.286
• Mol file: 81699-50-5.mol

Synonyms:

Chemical Property of ethyl 9H-fluorene-1-carboxylate

Chemical Property:

Purity/Quality:

ETHYL 9H-FLUORENE-1-CARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 9H-fluorene-1-carboxylate

There total 4 articles about ethyl 9H-fluorene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-oxo-9H-fluorene-1-carboxylic acid (1573-92-8) → fluorene-1-carboxylic acid ethyl ester (81699-50-5)

Guidance literature:

Multi-step reaction with 2 steps

1: water; sodium amalgam

2: HCl

With hydrogenchloride; sodium amalgam; water;

Reference yield:

fluoranthene (206-44-0) → fluorene-1-carboxylic acid ethyl ester (81699-50-5)

Guidance literature:

Multi-step reaction with 3 steps

1: CrO₃; acetic acid

2: sodium hydroxide; trimethylene glycol; aqueous hydrazine hydrate / 205 °C

3: ethanol; hydrogen chloride

With chromium(VI) oxide; hydrogenchloride; sodium hydroxide; ethanol; hydrazine hydrate; acetic acid; trimethyleneglycol;

DOI:10.1021/ja01171a502

Reference yield:

9H-fluorene-1-carboxylic acid (6276-03-5) → fluorene-1-carboxylic acid ethyl ester (81699-50-5)

Guidance literature:

With hydrogenchloride; ethanol;

DOI:10.1021/ja01171a502

upstream raw materials:

ethanol

9H-fluorene-1-carboxylic acid

9-oxo-9H-fluorene-1-carboxylic acid

fluoranthene