N2-Cyclohexylidenebenzhydrazide

Base Information

• Chemical Name: N2-Cyclohexylidenebenzhydrazide
• CAS No.: 24214-79-7
• Molecular Formula: C13H16 N2 O
• Molecular Weight: 216.283
• Hs Code.: 2928000090
• Mol file: 24214-79-7.mol

Synonyms:Benzoicacid, cyclohexylidenehydrazide (6CI,8CI,9CI); Cyclohexanone benzoylhydrazone;NSC 148501

Chemical Property of N2-Cyclohexylidenebenzhydrazide

Chemical Property:

• PSA: 41.46000
• Density: 1.12g/cm3
• LogP: 3.12740

Purity/Quality:

99% ^*data from raw suppliers

N''-cyclohexylidenebenzohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N2-Cyclohexylidenebenzhydrazide

There total 2 articles about N2-Cyclohexylidenebenzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + benzoic acid hydrazide (613-94-5) → cyclohexanone benzoylhydrazone (24214-79-7)

Guidance literature:

at 152 ℃; for 0.0833333h; under 3750.38 Torr; Microwave irradiation; neat (no solvent);

DOI:10.1021/cc9001444

Reference yield:

→ cyclohexanone benzoylhydrazone (24214-79-7)

Guidance literature:

Aus Bezoylhydrazin, Cyclohexanon in EtOH beim Erhitzen;

Reference yield: 100.0%

cyclohexanone benzoylhydrazone (24214-79-7) + methanol (67-56-1) → 2,2-pentamethylene-5-methoxy-5-phenyl-1,3,4-Δ3-oxadiazoline (138723-84-9)

Guidance literature:

With [bis(acetoxy)iodo]benzene; at 0 ℃; for 0.0333333h;

DOI:10.1021/jo00064a027

upstream raw materials:

cyclohexanone

benzoic acid hydrazide

Downstream raw materials:

4-acetyl-5,5-pentamethylene-2-phenyl-1,3,5-oxadiazoline

3-acetoxy-3-phenyl-4-oxa-1,2-diaza-spiro[4.5]dec-1-ene

2,2-pentamethylene-5-methoxy-5-phenyl-1,3,4-Δ³-oxadiazoline

1-(1-Cyanocyclohexyl)-2-benzoylhydrazine